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Journal Articles

Rapid analytical method of $$^{90}$$Sr in urine sample; Rapid separation of Sr by phosphate co-precipitation and extraction chromatography, followed by determination by triple quadrupole inductively coupled plasma mass spectrometry (ICP-MS/MS)

Tomita, Jumpei; Takeuchi, Erina

Applied Radiation and Isotopes, 150, p.103 - 109, 2019/08

 Times Cited Count:14 Percentile:82.61(Chemistry, Inorganic & Nuclear)

A rapid analytical method for determining $$^{90}$$Sr in urine samples (1-2 L) was developed to assess the internal exposure of workers in a radiological emergency. Strontium in a urine sample was rapidly separated by phosphate co-precipitation, followed by extraction chromatography with a tandem column of Pre-filter, TRU and Sr resin, and the $$^{90}$$Sr activity was determined by ICP-MS/MS. Measurement in the MS/MS mode with an O$$_{2}$$ reaction gas flow rate 1 mL min$$^{-1}$$ showed no tailing of $$^{88}$$Sr at m/z = 90 up to 50 mg-Sr L$$^{-1}$$. The interferences of Ge, Se and Zr at m/z = 90 were successfully removed by chemical separation. This analytical method was validated by the results of the analyses of synthetic urine samples (1.2-1.6 L) containing a known amount of $$^{90}$$Sr along with 1 mg of each of Ge, Se, Sr and Zr. The turnaround time for analysis was about 10 h, and the detection limit of $$^{90}$$Sr was approximately 1 Bq per urine sample.

Journal Articles

Recent trend of the radionuclide analyses in bioassay

Tomita, Jumpei

Bunseki, 2019(3), p.112 - 113, 2019/03

no abstracts in English

Journal Articles

Tacticity, molecular weight, and molecular-weight-distribution relationships in stereoregular polyacrilonitrile prepared by electron beam irradiation canal polymerization

Minagawa, Masatomo*; Okada, Yasushi*; Nouchi, Kentaro*; Sato, Yasuhiko*; Yoshii, Fumio

Colloid and Polymer Science, 278(8), p.757 - 763, 2000/08

no abstracts in English

Journal Articles

Kinetic investigation of the reaction of pertechnetate with thiourea derivatives

Hashimoto, Kazuyuki; *

Technetium, Rhenium and Other Metals in Chemistry and Nuclear Medicine, p.325 - 328, 1999/00

no abstracts in English

JAEA Reports

Reutilization system of carbon dioxide using nuclear heat

Fumizawa, Motoo; Inaba, Yoshitomo; Hishida, Makoto; Ogawa, Masuro; *

JAERI-Tech 96-022, 82 Pages, 1996/06

JAERI-Tech-96-022.pdf:2.2MB

no abstracts in English

Journal Articles

Application of neutron-induced prompt gamma-ray analysis for determination of B-10 in BNCT

Yonezawa, Chushiro; ; Sawahata, Hiroyuki*; *; Hoshi, Michio; Ito, Yasuo*

Cancer Neutron Capture Therapy, 0, p.221 - 225, 1996/00

no abstracts in English

Journal Articles

Stability of guest molecules in urea canal complexes by canal polymerization

Yoshii, Fumio; Makuuchi, Keizo

JAERI-Conf 95-003, p.584 - 587, 1995/03

no abstracts in English

Journal Articles

Solvent extraction of technetium in urine with TBP

; Hashimoto, Kazuyuki

Journal of Radioanalytical and Nuclear Chemistry, Letters, 201(5), p.361 - 370, 1995/00

no abstracts in English

Journal Articles

In vivo glycation of diabetic tendon collagen studied by neutron diffraction

Niimura, Nobuo*

Farumashia, 30(4), p.400 - 401, 1994/04

no abstracts in English

Journal Articles

Kinetic investigation of the reaction of pertechnetate with thiourea in a hydrochloric acid solution

Hashimoto, Kazuyuki; *

Journal of Radioanalytical and Nuclear Chemistry, Letters, 188(6), p.391 - 400, 1994/00

no abstracts in English

Journal Articles

Stability of guest molecules in urea canal complexes by canal polymerization

Yoshii, Fumio; Makuuchi, Keizo

Macromolecular Reports, A30(SUPPL.1-2), p.127 - 135, 1993/00

no abstracts in English

Journal Articles

Reactions of technetium(III)-thiourea derivative complexes with pyrimidine derivatives

Hashimoto, Kazuyuki; Kudo, Hiroshi; *; *

Radiochimica Acta, 63, p.167 - 171, 1993/00

no abstracts in English

Journal Articles

Formation of Tc(III) complexes with EDTA and HEDTA

Hashimoto, Masashi; *; *; *

Radiochimica Acta, 63, p.173 - 177, 1993/00

no abstracts in English

JAEA Reports

None

PNC TJ1262 92-001, 96 Pages, 1992/02

PNC-TJ1262-92-001.pdf:2.71MB

None

Journal Articles

Trailing effect of urea canal complex and its application

Yoshii, Fumio; Makuuchi, Keizo

Zairyo Gijutsu, 10(9), p.280 - 288, 1992/00

no abstracts in English

Journal Articles

Dissolution behavior of highly isotactic polyacrylonitrile in N, N-dimethylformamide at an elevated temperature

*; *; *; Yoshii, Fumio

Macromolecules, 22(5), p.2054 - 2058, 1989/00

 Times Cited Count:22 Percentile:72.35(Polymer Science)

no abstracts in English

Journal Articles

A Test to enhance the excretion of tritium in man by excessive water intake

; ; ;

Health Physics, 41(6), p.825 - 828, 1981/00

no abstracts in English

Journal Articles

Post-polymerization of long chain monomers $$gamma$$-irradiated in urea canal complexes by addition of various solvents

Yoshii, Fumio; Kaetsu, Isao

Kobunshi Rombunshu, 36(1), p.61 - 63, 1979/01

 Times Cited Count:0

Post-polymerization by the addition of various solvents to long chain monomers after irradiation in the urea canal complexes was investigatThe polymerization occurred nearly quantitatively by the addition of highly viscous solvents, more easily than by the addition of cooled methanol. This post-polymerization occurs when the monomers are released by the dissolution of the urea canal. It is deduced that the decreased termination rate and the increased life-time of growing chain radicals in high viscosity solvents increase the polymerizability of monomers.

Journal Articles

Journal Articles

Monitoring experiences of tritium in JAERI

; Yabe, Akira; Kishida, Masami

Proc.Int.Symp.on Behaviour of Tritium in the Environment, p.613 - 622, 1979/00

no abstracts in English

35 (Records 1-20 displayed on this page)